Výzkumné články [Research articles]
25. Paškanová, N.; Hlavatá, P.; Jurásek, B.; Kuchař, M.; Kohout, M. Tuning Parameters of Single Quadrupole Mass Detector Hyphenated to Supercritical Fluid Chromatography for Enantioseparation of Synthetic Cathinones. J. Chromatogr. Open 2024, 5, 100139.
DOI: https://doi.org/10.1016/j.jcoa.2024.100139
24. Jurásek, B.; Fagan, P.; Dolenský, B.; Paškanová, N.; Dobšíková, K.; Raich, I.; Jurok, R.; Setnička, V.; Kohout, M.; Čejka, J.; Kuchař, M. A Structural Spectroscopic Study of Dissociative Anaesthetic Methoxphenidine. New J. Chem. 2023, 47 (9), 4543–4551.
DOI: https://doi.org/10.1039/D2NJ06126K
23. Jurásek, B.; Rimpelová, S.; Babor, M.; Čejka, J.; Bartůněk, V.; Kuchař, M. Intriguing Cytotoxicity of the Street Dissociative Anesthetic Methoxphenidine: Unexpected Impurities Spotted. Int. J. Mol. Sci. 2022, 23 (4), 2083.
DOI: https://doi.org/10.3390/ijms23042083
22. Štefková‐Mazochová, K.; Danda, H.; Dehaen, W.; Jurásek, B.; Šíchová, K.; Pinterová‐Leca, N.; Mazoch, V.; Krausová, B. H.; Kysilov, B.; Smejkalová, T.; Vyklický, L.; Kohout, M.; Hájková, K.; Svozil, D.; Horsley, R. R.; Kuchař, M.; Páleníček, T. Pharmacokinetic, Pharmacodynamic, and Behavioural Studies of Deschloroketamine in Wistar Rats. Br. J. Pharmacol. 2022, 179 (1), 65–83.
DOI: https://doi.org/10.1111/bph.15680
21. Nykodemová, J.; Šuláková, A.; Palivec, P.; Češková, H.; Rimpelová, S.; Šíchová, K.; Leonhardt, T.; Jurásek, B.; Hájková, K.; Páleníček, T.; Kuchař, M. 2C-B-Fly-NBOMe Metabolites in Rat Urine, Human Liver Microsomes and C. Elegans: Confirmation with Synthesized Analytical Standards. Metabolites 2021, 11 (11), 775.
DOI: https://doi.org/10.3390/metabo11110775
20. Spálovská, D.; Paškan, M.; Jurásek, B.; Kuchař, M.; Kohout, M.; Setnička, V. Structural Spectroscopic Study of Enantiomerically Pure Synthetic Cathinones and Their Major Metabolites. New J. Chem. 2021, 45 (2), 850–860.
DOI: https://doi.org/10.1039/D0NJ05065B
19. Shishkanova, T. V.; Štěpánková, N.; Tlustý, M.; Tobrman, T.; Jurásek, B.; Kuchař, M.; Trchová, M.; Fitl, P.; Vrňata, M. Electrochemically Oxidized 15-Crown-5 Substituted Thiophene and Host-Guest Interaction with New Psychoactive Substances. Electrochim. Acta 2021, 373, 137862.
DOI: https://doi.org/10.1016/j.electacta.2021.137862
18. Jurásek, B.; Čmelo, I.; Svoboda, J.; Čejka, J.; Svozil, D.; Kuchař, M. New Psychoactive Substances on Dark Web Markets: From Deal Solicitation to Forensic Analysis of Purchased Substances. Drug Test. Anal. 2021, 13 (1), 156–168.
DOI: https://doi.org/10.1002/dta.2901
17. Shishkanova, T. V.; Vatrsková, L.; Spálovská, D.; Králík, F.; Cuřínová, P.; Winkler, M.; Budka, J.; Jurásek, B.; Kuchař, M.; Setnička, V. Complexation of Cathinones by 4-Tert-Butylcalix[4]Arene Tetra-Acetate as a Possible Technique for Forensic Analysis. Forensic Toxicol. 2020, 38 (1), 70–78.
DOI: https://doi.org/10.1007/s11419-019-00489-8
16. Kolderová, N.; Jurásek, B.; Kuchař, M.; Lindner, W.; Kohout, M. Gradient Supercritical Fluid Chromatography Coupled to Mass Spectrometry with a Gradient Flow of Make-up Solvent for Enantioseparation of Cathinones. J. Chromatogr. A 2020, 1625, 461286.
DOI: https://doi.org/10.1016/j.chroma.2020.461286
15. Jurásek, B.; Bartůněk, V.; Huber, Š.; Fagan, P.; Setnička, V.; Králík, F.; Dehaen, W.; Svozil, D.; Kuchař, M. Can X-Ray Powder Diffraction Be a Suitable Forensic Method for Illicit Drug Identification? Front. Chem. 2020, 8.
DOI: https://doi.org/10.3389/fchem.2020.00499
14. Hájková, K.; Jurásek, B.; Čejka, J.; Štefková, K.; Páleníček, T.; Sýkora, D.; Kuchař, M. Synthesis and Identification of Deschloroketamine Metabolites in Rats’ Urine and a Quantification Method for Deschloroketamine and Metabolites in Rats’ Serum and Brain Tissue Using Liquid Chromatography Tandem Mass Spectrometry. Drug Test. Anal. 2020, 12 (3), 343–360.
DOI: https://doi.org/10.1002/dta.2726
13. Jurásek, B.; Čmelo, I.; Hájková, K.; Kofroňová, E.; Kuchař, M. Counterfeit Benzodiazepines—A Phantom Menace. Int. J. Clin. Pract. 2020, 74 (10), e13575.
DOI: https://doi.org/10.1111/ijcp.13575
12. Jurásek, B.; Bartůněk, V.; Huber, Š.; Kuchař, M. X-Ray Powder Diffraction – A Non-Destructive and Versatile Approach for the Identification of New Psychoactive Substances. Talanta 2019, 195, 414–418.
DOI: https://doi.org/10.1016/j.talanta.2018.11.063
11. Spálovská, D.; Králík, F.; Kohout, M.; Jurásek, B.; Habartová, L.; Kuchař, M.; Setnička, V. Structure Determination of Butylone as a New Psychoactive Substance Using Chiroptical and Vibrational Spectroscopies. Chirality 2018, 30 (5), 548–559.
DOI: https://doi.org/10.1002/chir.22825
10. Jurasek, B.; Babor, M.; Huber, S.; Kuchar, M. X-Ray Powder Diffraction Data for Methoxmetamine Hydrochloride, C14H20ClNO2. Powder Diffr. 2018, 33 (3), 242–245.
DOI: https://doi.org/10.1017/S0885715618000532
9. Jurásek, B.; Králík, F.; Rimpelová, S.; Čejka, J.; Setnička, V.; Ruml, T.; Kuchař, M.; Kohout, M. Synthesis, Absolute Configuration and in Vitro Cytotoxicity of Deschloroketamine Enantiomers: Rediscovered and Abused Dissociative Anaesthetic. New J. Chem. 2018, 42 (24), 19360–19368.
DOI: https://doi.org/10.1039/C8NJ03107J
8. Blastik, Z. E.; Voltrová, S.; Matoušek, V.; Jurásek, B.; Manley, D. W.; Klepetářová, B.; Beier, P. Azidoperfluoroalkanes: Synthesis and Application in Copper(I)-Catalyzed Azide-Alkyne Cycloaddition. Angew. Chem. Int. Ed. 2017, 56 (1), 346–349.
DOI: 10.1002/anie.201609715
7. Maixner, J.; Jurásek, B.; Himl, M.; Kuchař, M.; Babor, M. X-Ray Powder Diffraction Data for Methoxetamine Hydrochloride, C15H22ClNO2. Powder Diffr. 2017, 32 (04), 265–267.
DOI: https://doi.org/10.1017/S0885715617000860
6. Maixner, J.; Jurásek, B.; Kohout, M.; Kuchař, M.; Kačer, P. X-Ray Powder Diffraction Data for (S)-Deschloroketamine Hydrochloride, C13H18ClNO. Powder Diffr. 2017, 32 (03), 193–195.
DOI: https://doi.org/10.1017/S0885715617000586
5. Jurasek, B.; Himl, M.; Jurok, R.; Hajkova, K.; Vobinuskova, A.; Rezanka, P.; Kuchar, M. Synthesis of Methoxetamine, Its Metabolites and Deuterium Labelled Analog as Analytical Standards and Their HPLC and Chiral Capillary Electrophoresis Separation. RSC Adv. 2017, 7 (89), 56691–56696.
DOI: https://doi.org/10.1039/C7RA10893A
4. Hajkova, K.; Jurasek, B.; Sykora, D.; Palenicek, T.; Miksatkova, P.; Kuchar, M. Salting-out-Assisted Liquid–Liquid Extraction as a Suitable Approach for Determination of Methoxetamine in Large Sets of Tissue Samples. Anal. Bioanal. Chem. 2016, 408 (4), 1171–1181.
DOI: https://doi.org/10.1007/s00216-015-9221-1
3. Horsley, R. R.; Lhotkova, E.; Hajkova, K.; Jurasek, B.; Kuchar, M.; Palenicek, T. Detailed Pharmacological Evaluation of Methoxetamine (MXE), a Novel Psychoactive Ketamine Analogue—Behavioural, Pharmacokinetic and Metabolic Studies in the Wistar Rat. Brain Res. Bull. 2016, 126, 102–110.
DOI: https://doi.org/10.1016/j.brainresbull.2016.05.002
2. Chernykh, Y.; Jurásek, B.; Beier, P. Synthesis of Tetrafluoroethyl- and Tetrafluoroethylene-Containing Amines by the Reaction of Silanes with Enamines under Acidic Conditions. J. Fluor. Chem. 2015, 171, 162–168.
DOI: https://doi.org/10.1016/j.jfluchem.2014.08.004
1. Václavík, J.; Chernykh, Y.; Jurásek, B.; Beier, P. Nucleophilic Tetrafluoroethylation of Carbonyl Compounds with Fluorinated Sulfones. J. Fluor. Chem. 2015, 169, 24–31.
DOI: https://doi.org/10.1016/j.jfluchem.2014.10.019